Chromium Speciation Using Flow-injection Preconcentration on Xylenol Orange Functionalized Amberlite XAD-16 and Determination in Industrial Water Samples by Flame Atomic Absorption Spectrometry
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Preconcentration and speciation of chromium in water samples by atomic absorption spectrometry after cloud-point extraction.
A rapid, sensitive and accurate atomic absorption method for Cr(III) and Cr(VI) ions was developed based on the cloud-point extraction (CPE) technique. Cr(III) reacts with a new Schiff's base ligand to form the hydrophobic complex, which is subsequently entrapped in the surfactant micelles. The Cr(VI) assay is based on its reduction to Cr(III) by the addition of concentrated H2SO4 and ethanol t...
متن کاملPreconcentration and determination of palladium water samples by ionic liquid - dispersive liquid liquid microextraction combined with flame atomic absorption spectrometry
A simple, rapid and efficient dispersive liquid–liquid microextraction by use of ionic liquid (IL-DLLME)method, followed by flame atomic absorption spectrometry (FAAS) was developed for the preconcentrationand determination of palladium in water samples. In this method, an appropriate mixture of acetone and octylmethyl imidazolium hexafluorophosphate was injected rapidly into the aqueous sample...
متن کاملPreconcentration of lead with Amberlite XAD-2 and Amberlite XAD-7 based chelating resins for its determination by flame atomic absorption spectrometry.
Four chelating matrices prepared by coupling Amberlite XAD-2 with chromotropic acid (AXAD-2-CA or 1), pyrocatechol (AXAD-2-PC or 2) and thiosalicylic acid (AXAD-2-TSA or 3) through azo spacer and impregnation of Amberlite XAD-7 with xylenol orange (AXAD-7-XO or 4) have been studied for enrichment of lead(II). All the four resins quantitatively sorb Pb(II) at pH 3.0-8.0 when the flow rate is mai...
متن کاملDetermination of lead and cadmium in water samples by cloud point extraction prior to flame atomic absorption spectrometry determination
Pb and Cd in water samples were determined by cloud point extraction (CPE) with sodiumdiethyldithiocarbamate (DDTC) as the chelating agent and octylphenoxypolyethanl (Triton X-114) asthe surfactant prior to flame atomic absorption spectrometry (FAAS) determination. The main factorsof affecting the extraction and detection processes were optimized. The preconcentration of 10 mL ofstandard soluti...
متن کاملDetermination of beryllium in solid samples by flame atomic absorption spectrometry after preconcentration on activated carbon.
It is generally supposed that the preconcentration procedure is used for the determination of metal concentrations under the sensitivity of the measurement method. This study showed that preconcentration is also need for the beryllium (Be) concentration over the sensitivity of atomic absorption spectrometry. For this purpose, a simple and selective method for the determination of Be in solid sa...
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ژورنال
عنوان ژورنال: Analytical Sciences
سال: 2015
ISSN: 0910-6340,1348-2246
DOI: 10.2116/analsci.31.1303